Mechanical activation and silver supplementation as determinants of the antibacterial activity of titanium dioxide nanoparticles

Објеката

Тип
Рад у часопису
Верзија рада
објављена верзија
Језик
енглески
Креатор
Ljubica Anđelković, Marija Šuljagić, Vladimir Pavlović, Miljana Mirković, Boško Vrbica, Irena Novaković, Dalibor Stanković, Aleksandar Kremenović, Vuk Uskoković
Извор
Colloids and Surfaces A: Physicochemical and Engineering Aspects
Издавач
Elsevier BV
Датум издавања
2024
Сажетак
This study employed a novel synthetic approach involving a modified reverse co-precipitation
method utilizing glacial acetic acid to synthesize α-Bi2O3
. X-ray powder diffraction and scanning and
transmission electron microscopy analyses revealed the formation of a rod-like α-Bi2O3 microstructure. The prepared material was utilized to modify a glassy carbon paste (GCP) electrode for the
development of an electrochemical sensor for acetaminophen (APAP) detection using differential
pulse voltammetry (DPV). Cyclic voltammetry studies revealed that the GCP@Bi2O3 electrode exhibited enhanced electrochemical properties compared to the bare GCP. The designed GCP@Bi2O3
sensor detected APAP in the linear concentration range from 0.05 to 12.00 µM, with LOQ and LOD of
36 nM and 10 nM, respectively. Additionally, the developed sensor demonstrated sufficient precision,
repeatability, and selectivity toward APAP detection. The recovery values between the declared
and found APAP content in a pharmaceutical formulation (Caffetin®) displayed the advantageous
accuracy, precision, and applicability of the GCP@Bi2O3 sensor and the developed DPV method for
real-time APAP detection in pharmaceuticals, with minimal interference from the matrix effect.
том
691
Број
12(7)
почетак странице
122
doi
10.1016/j.colsurfa.2024.133890
issn
0927-7757
Subject
štapićasta a-Bi2O3 mikrostruktura, reverzna sinteza ko-precipitacije, elektrohemijski senzor, detekcija acetaminofena
rod-like α-Bi2O3 microstructure, reverse co-precipitation synthesis, electrochemical sensor, acetaminophen detection
Шира категорија рада
M20
Ужа категорија рада
М22
Права
Отворени приступ
Лиценца
Creative Commons – CC0 Public Domain
Формат
.pdf

Ljubica Anđelković, Marija Šuljagić, Vladimir Pavlović, Miljana Mirković, Boško Vrbica, Irena Novaković, Dalibor Stanković, Aleksandar Kremenović, Vuk Uskoković. "Mechanical activation and silver supplementation as determinants of the antibacterial activity of titanium dioxide nanoparticles" in Colloids and Surfaces A: Physicochemical and Engineering Aspects, Elsevier BV (2024). https://doi.org/10.1016/j.colsurfa.2024.133890

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